Medoks, G. V.’s team published research in Zhurnal Obshchei Khimii in 26 | CAS: 312-40-3

Zhurnal Obshchei Khimii published new progress about 312-40-3. 312-40-3 belongs to catalysis-chemistry, auxiliary class Organic Silicones, name is Difluorodiphenylsilane, and the molecular formula is C12H10F2Si, Application of Difluorodiphenylsilane.

Medoks, G. V. published the artcileReaction of phenylmagnesium bromide with silicon tetrafluoride, Application of Difluorodiphenylsilane, the publication is Zhurnal Obshchei Khimii (1956), 113-15, database is CAplus.

Passage of SiF4 into PhMgBr solution from 70.6 g. PhBr with ice cooling gave a reaction mixture which formed 2 liquid layers and some solid; after 24 hrs. the mixture was treated with cooling with 11% HCl, yielding 2.73 g. Ph2SiF2, b28 247-8¡ã (2.48 g. of less pure product also formed), and 59.5% Ph3SiF, b30 245-50¡ã, m. 64¡ã. PhMgBr from 2.57 g. Mg was treated with SiF4 as above for 20 min., and the 2-layered mixture was treated with an equal amount of PhMgBr solution as above, freed of Et2O, and heated 1 hr. at 175-80¡ã, yielding after usual treatment 8.4 g. Ph4Si (I), m. 230.5¡ã. In 5 days at room temperature PhMgBr and Ph3SiF (4.17 g.) gave 0.85 g. I; at 180-2¡ã a 93% yield was obtained.

Zhurnal Obshchei Khimii published new progress about 312-40-3. 312-40-3 belongs to catalysis-chemistry, auxiliary class Organic Silicones, name is Difluorodiphenylsilane, and the molecular formula is C12H10F2Si, Application of Difluorodiphenylsilane.

Referemce:
https://courses.lumenlearning.com/boundless-chemistry/chapter/catalysis/,
Catalysis – Wikipedia