Yakan, Hasan’s team published research in Monatshefte fuer Chemie in 149 | CAS: 19117-31-8

Monatshefte fuer Chemie published new progress about 19117-31-8. 19117-31-8 belongs to catalysis-chemistry, auxiliary class Oxidant, name is N-(tert-Butyl)-S-phenylthiohydroxylamine, and the molecular formula is C10H15NS, HPLC of Formula: 19117-31-8.

Yakan, Hasan published the artcileComparison of conventional and microwave-assisted synthesis of some new sulfenamides under free catalyst and ligand, HPLC of Formula: 19117-31-8, the publication is Monatshefte fuer Chemie (2018), 149(11), 2047-2057, database is CAplus.

Sulfenamides were prepared in 70-98% yields by treatment of N-arylthio- and N-alkylthiophthalimides with cyclohexylamine, morpholine, or pyrrolidine in ¦Â-ethoxyethanol under microwave irradiation; the yields of sulfenamides using microwave irradiation and using conventional heating were compared. Tert-butylamine, aniline, benzylamine, 1-hexylamine, ethanolamine, diethylamine, N-methyl-1-butanamine, N-ethylaniline, and N-methylbenzylamine did not yield the desired sulfenamides on reaction with N-arylthio or N-alkylthiophthalimides, but yielded only disulfides. The reaction was not inhibited by radical inhibitors. The N-arylthio and N-alkylthiophthalimides were prepared from the corresponding thiols and phthalimide with Br2 in pyridine/acetonitrile.

Monatshefte fuer Chemie published new progress about 19117-31-8. 19117-31-8 belongs to catalysis-chemistry, auxiliary class Oxidant, name is N-(tert-Butyl)-S-phenylthiohydroxylamine, and the molecular formula is C10H15NS, HPLC of Formula: 19117-31-8.

Referemce:
https://courses.lumenlearning.com/boundless-chemistry/chapter/catalysis/,
Catalysis – Wikipedia